**Acknowledgements**

This study was financially supported by Proyects MAT2017-83825-C4-1-R from MINECO and Y2018/NMT-4668 from CAM, Spain. The authors would like to thank Antonio Tomás, Dr. Judit Caballero, and Prof. Paloma Adeva from Electron Microscopy Lab of CENIM for their support and help with the microstructure characterization and Edurne Laurín for her help in TEM sample preparation.

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