**Author details**

Ayi A. Ayi\*, Providence B. Ashishie, Emmanuel E. Khansi, Joseph O. Ogar, Chinyere A. Anyama and Bassey E. Inah Inorganic Materials Research Laboratory, Department of Pure and Applied Chemistry, University of Calabar, Calabar, Nigeria

\*Address all correspondence to: ayiayi72@gmail.com

© 2020 The Author(s). Licensee IntechOpen. This chapter is distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/ by/3.0), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.

**17**

*Nano/Micro-Structured Materials: Synthesis, Morphology and Applications*

[10] Kitamura Y, Okinaka N, Shibayama T, Mahaney OOP, Kusano D, Ohtani B, et al. Combustion synthesis of TiO2 nanoparticles as photocatalyst. Powder

Technology. 2007;**176**:93-98

Physics. 2003;**36**:R80-R95

Research. 2004;**6**:193-207

2014;**42**:27-37

[11] Jones AC, Chalker PR. Some recent developments in the chemical vapour deposition of electroceramics ocides. Journal of Physics D: Applied

[12] Wang W, Lenggoro IW, Terashi Y, Kim TO, Okuyama K. One step synthesis of titanium oxide nanoparticles by spray pyrolysis of organic precursors. Materials Science and Engineering B. 2005;**123**:194-202

[13] Watson S, Beydoun D, Scott J, Amal R. Preparation of nanosized cryrstalline TiO2 particles at low temperature for photocatalysis. Journal of Nanoparticle

[14] Douglas G, Shackleton M, Woods P. Hydrotalcite formation facilitates effective contaminant and radionuclide removal from acidic uranium mine barren lixiviant. Applied Geochemistry.

[15] Douglas G. Contaminant removal from acidic mine pit water via in situ hydrotalcite formation. Applied

[16] Balsamo N, Mendieta S, Olivab M, Eimer G, Crivello M. Synthesis and characterization of metal mixed oxides from layered double hydroxides. Procedia

Materials Science. 2012;**1**:506-513

Catalysis Today. 1991;**11**:173-301

[17] Cavani F, Trifiròa F, Vaccaria A. Hydrotalcite-type anionic clays:

Preparation, properties and applications.

[18] Rives V. Layered Double Hydroxides: Present and Future. New York, NY, USA: Nova Science Publishers; 2001

Geochemistry. 2014;**51**:15-22

*DOI: http://dx.doi.org/10.5772/intechopen.85698*

[1] Caruso F, editor. Colloids and Colloid Assemblies: Synthesis, Modification, Organization and Utilization of Colloid Particles. Weinheim: Wiley VCH; 2004

[2] Goldenberg S. Dispersant 'May Make Deep-Water Horizon Oil Spill more Toxic'. The Guardian Newspaper. 5 May 2010

[3] Zahir F, Rizwi SJ, Haq SK, Khan RH. Low dose mercury toxicity and human health. Environmental Toxicology and Pharmacology. 2005;**20**:351-360

[4] USEP Agency. Nanotechnology for site remediation fact sheet. 2009

[5] Moffat G, Williams RA, Webb C, Stirling R. Selective separations in environmental and industrial processes using magnetic carrier technology. Minerals Engineering.

[6] Ashishie PB, Inah BE, Ayi AA. Evaluation of antimicrobial activity of ionic liquid-assisted synthesis of monometallic silver and bimetallic copper-silver nanoparticles. International Journal of Sciences. 2018;**7**(5):25-31

[7] Khansi EE, Anyama CA, Ayi AA, Onwuka JC. Use of nanostructured layered double hydroxides as nano filters in the removal of Fe2+ and Ca2+ ions from oil wells. Advances in Materials Science and Engineering. 2018;**2018**:1-7.

DOI: 10.1155/2018/5306825

1995;**7**:663-671

2009;**C113**:13593-13599

[8] Cheng H, Ma J, Zhao Z, Qi L. Hydrothermal preparation of uniform nanosize rutile and anatase particles. Chemistry of Materials.

[9] Ge S, Shi X, Sun K, Li C, Uher C, Baker JR, et al. Facile hydrothermal synthesis of iron oxide nanoparticles with tunable magnetic properties. The Journal of Physical Chemistry.

1994;**7**(8):1039-1056

**References**

*Nano/Micro-Structured Materials: Synthesis, Morphology and Applications DOI: http://dx.doi.org/10.5772/intechopen.85698*
